Regio- and chemoselective metalation of arenes and heteroarenes using hindered metal amide bases (Q37939746)

25 August 2017

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title

Regio- and chemoselective metalation of arenes and heteroarenes using hindered metal amide bases (English)

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25 August 2017

5

Paul Knochel

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25 August 2017

Benjamin Haag

1

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25 August 2017

Marc Mosrin

series ordinal

2

1 reference

25 August 2017

Hiriyakkanavar Ila

series ordinal

3

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25 August 2017

Vladimir Malakhov

series ordinal

4

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25 August 2017

language of work or name

English

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publication date

27 September 2011

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Angewandte Chemie International Edition

25 August 2017

published in

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volume

50

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25 August 2017

issue

42

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25 August 2017

page(s)

9794-9824

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Recent advances in the chemistry and biology of naturally occurring antibiotics

25 August 2017

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Palladium-catalyzed direct arylation of azine and azole N-oxides: reaction development, scope and applications in synthesis

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Aryl-aryl bond formation by transition-metal-catalyzed direct arylation.

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All-carbon quaternary centers via ruthenium-catalyzed hydroxymethylation of 2-substituted butadienes mediated by formaldehyde: beyond hydroformylation

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Enantioselective iridium-catalyzed carbonyl allylation from the alcohol or aldehyde oxidation level via transfer hydrogenative coupling of allyl acetate: departure from chirally modified allyl metal reagents in carbonyl addition

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The atom economy--a search for synthetic efficiency

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Directed ortho metalation. Tertiary amide and O-carbamate directors in synthetic strategies for polysubstituted aromatics

21 January 2018

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Beyond thermodynamic acidity: a perspective on the complex-induced proximity effect (CIPE) in deprotonation reactions

21 January 2018

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Functionalization of diazines and benzo derivatives through deprotonated intermediates

21 January 2018

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The 2 x 3 toolbox of organometallic methods for regiochemically exhaustive functionalization

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Alpha-fluorinated ethers, thioethers, and amines: anomerically biased species.

21 January 2018

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Deprotonative metalation using ate compounds: synergy, synthesis, and structure building

21 January 2018

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Avant-garde metalating agents: structural basis of alkali-metal-mediated metalation

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Highly functionalized organomagnesium reagents prepared through halogen-metal exchange

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Preparation of functionalized aryl magnesium reagents by the addition of magnesium aryl thiolates and amides to arynes

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Aromatic organolithium reagents bearing electrophilic groups. Preparation by halogen-lithium exchange

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Preparation of Highly Functionalized Grignard Reagents by an Iodine-Magnesium Exchange Reaction and its Application in Solid-Phase Synthesis.

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Efficient Synthesis of Functionalized Organozinc Compounds by the Direct Insertion of Zinc into Organic Iodides and Bromides

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Iron-Catalyzed Cross-Coupling Reactions

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A LiCl-Mediated Br/Mg Exchange Reaction for the Preparation of Functionalized Aryl- and Heteroarylmagnesium Compounds from Organic Bromides

21 January 2018

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Catalysts for Suzuki-Miyaura coupling processes: scope and studies of the effect of ligand structure

21 January 2018

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Negishi cross-couplings of unsaturated halides bearing relatively acidic hydrogen atoms with organozinc reagents.

21 January 2018

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Metalation as a Side Reaction in the Preparation of Organolithium Compounds

21 January 2018

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Carbamoyl translocations by an anionic ortho-fries and cumulenolate alpha-acylation pathway: regioselective synthesis of polysubstituted chromone 3- and 8-carboxamides

21 January 2018

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CF(3)-bearing aromatic and heterocyclic building blocks

21 January 2018

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Buttressing effects on haloarene deprotonation: a merely kinetic or also thermodynamic phenomenon?

21 January 2018

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An improved method for the bromination of metalated haloarenes via lithium, zinc transmetalation: a convenient synthesis of 1,2-dibromoarenes.

21 January 2018

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New, improved procedure for the synthesis of structurally diverse N-spiro C2-symmetric chiral quaternary ammonium bromides.

21 January 2018

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Pyridine elaboration through organometallic intermediates: regiochemical control and completeness

21 January 2018

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21 January 2018

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An Unprecedented Hexapotassium-Hexamagnesium 24-Membered Macrocyclic Amide: A Polymetallic Cationic Host to Six Monodeprotonated Arene Anions This work was supported by the UK Engineering and Physical Science Research Council (Grant award No. GR/M78

21 January 2018

1 reference

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Regio- and chemoselective direct generation of functionalized aromatic aluminum compounds using aluminum ate base

21 January 2018

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Deprotonative metalation of functionalized aromatics using mixed lithium-cadmium, lithium-indium, and lithium-zinc species

21 January 2018

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Direct C-H metalation with chromium(II) and iron(II): transition-metal host/benzenediide guest magnetic inverse-crown complexes.

21 January 2018

1 reference

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Alkali-metal-mediated manganationII of functionalized arenes and applications of ortho-manganated products in Pd-catalyzed cross-coupling reactions with iodobenzene.

21 January 2018

1 reference

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Generation of functionalized asymmetric benzynes with TMP-zincates. Effects of ligands on selectivity and reactivity of zincates

21 January 2018

1 reference

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Generation and suppression of 3-/4-functionalized benzynes using zinc ate base (TMP-Zn-ate): new approaches to multisubstituted benzenes.

21 January 2018

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Closer insight into the reactivity of TMP-dialkyl zincates in directed ortho-zincation of anisole: experimental evidence of amido basicity and structural elucidation of key reaction intermediates

21 January 2018

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Isolation and structural elucidation of a key aluminoaromatic intermediate and evidence for dismutation phenomena in TMP-alumination chemistry.

21 January 2018

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Selective meta-deprotonation of toluene by using alkali-metal-mediated magnesiation

21 January 2018

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Developing a hetero-alkali-metal chemistry of 2,2,6,6-tetramethylpiperidide (TMP): stoichiometric and structural diversity within a series of lithium/sodium, lithium/potassium and sodium/potassium TMP compounds

21 January 2018

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Isolation and characterisation of the mixed-metal alkyl amide [(TMEDA)Na(mu-Bu)(mu-TMP)Mg(TMP)], an unexpected chelate-trapped intermediate in the formation of inverse crowns

21 January 2018

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Komplexbildung und Reaktivität in der metallorganischen Chemie

21 January 2018

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Building an extended inverse crown motif via alkali-metal-mediated alpha-magnesiation of furan

21 January 2018

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Regioselective Tetrametalation of Ferrocene in a Single Reaction: Extension of s-Block Inverse Crown Chemistry to the d-Block This work was supported by the UK Engineering and Physical Science Research Council through grant award no GR/M78113.

21 January 2018

1 reference

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A homologous series of regioselectively tetradeprotonated group 8 metallocenes: new inverse crown ring compounds synthesized via a mixed sodium-magnesium tris(diisopropylamide) synergic base

21 January 2018

1 reference

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Sodium dialkyl-amidozincates: alkyl or amido bases? An experimental and theoretical case study

21 January 2018

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Pre-Metalation Structural Insights into the Use of Alkali-Metal-Mediated Zincation for Directedortho-Metalation of a Tertiary Aromatic Amide

21 January 2018

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Directedmeta-Metalation Using Alkali-Metal-Mediated Zincation

21 January 2018

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Synthetic and structural insights into the zincation of toluene: direct synergic ring metallation versus indirect nonsynergic lateral metallation

21 January 2018

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Structurally-defined potassium-mediated regioselective zincation of amino- and alkoxy-substituted pyridines

21 January 2018

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Structurally defined potassium-mediated zincation of pyridine and 4-R-substituted pyridines (R = Et, iPr, tBu, Ph, and Me2N) by using dialkyl-TMP-zincate bases

21 January 2018

1 reference

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Structure and Reaction Pathway of TMP-Zincate: Amido Base or Alkyl Base?

21 January 2018

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On the kinetic and thermodynamic reactivity of lithium di(alkyl)amidozincate bases in directed ortho metalation

21 January 2018

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Highly enantioselective hydrophosphonylation of aldehydes catalyzed by tridentate Schiff base aluminum(III) complexes

21 January 2018

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Catalytic, efficient, and syn-selective construction of deoxypolypropionates and other chiral compounds via Zr-catalyzed asymmetric carboalumination of allyl alcohol

21 January 2018

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All-catalytic, efficient, and asymmetric synthesis of alpha,omega-diheterofunctional reduced polypropionates via "one-pot" Zr-catalyzed asymmetric carboalumination-Pd-catalyzed cross-coupling tandem process

21 January 2018

1 reference

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Catalytic enantioselective Pudovik reaction of aldehydes and aldimines with tethered bis(8-quinolinato) (TBOx) aluminum complex.

21 January 2018

1 reference

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An Aluminum Ate Base: Its Design, Structure, Function, and Reaction Mechanism

21 January 2018

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Mixed alkylamido aluminate as a kinetically controlled base

21 January 2018

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Direct ortho cupration: a new route to regioselectively functionalized aromatics

21 January 2018

1 reference

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Deprotonative cadmation of functionalized aromatics

21 January 2018

1 reference

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Deprotonative magnesation and cadmation of [1,2,3]triazolo[1,5-a]pyridines.

21 January 2018

1 reference

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Direct metalation of heteroaromatic esters and nitriles using a mixed lithium-cadmium base. Subsequent conversion to dipyridopyrimidinones

21 January 2018

1 reference

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Lithium cadmate-mediated deprotonative metalation of anisole: experimental and computational study.

21 January 2018

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Coupling of Grignard Reagents with Organic Halides

21 January 2018

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Vinylation of Grignard reagents. Catalysis by iron

21 January 2018

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Contra-Friedel–Crafts tert-butylation of substituted aromatic rings via directed metallation and sulfinylation

21 January 2018

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Preparation of functionalized cyclic enol phosphates by halogen-magnesium exchange and directed deprotonation reactions

21 January 2018

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2,3-Functionalization of furans, benzofurans and thiophenes via magnesiation and sulfoxide-magnesium exchange.

21 January 2018

1 reference

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The first example of alpha-thiomagnesiums generated from dithioacetal monoxides with Grignard reagent; their properties and some synthetic applications

21 January 2018

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Advances in molecular design and synthesis of regioregular polythiophenes.

21 January 2018

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Removal of fluorine from and introduction of fluorine into polyhalopyridines: an exercise in nucleophilic hetarenic substitution.

21 January 2018

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Luminescent digold ethynyl thienothiophene and dithienothiophene complexes; their synthesis and structural characterisation

21 January 2018

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Preparation and selective reactions of mixed bimetallic aromatic and heteroaromatic boron-magnesium reagents

21 January 2018

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An extremely active catalyst for the Negishi cross-coupling reaction

21 January 2018

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Phosphorodiamidate-directed metalation of N-heterocycles using Mg- and Zn-TMP bases.

21 January 2018

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Regio- and chemoselective metalation of chloropyrimidine derivatives with TMPMgCl x LiCl and TMP(2)Zn x 2 MgCl(2) x 2 LiCl

21 January 2018

1 reference

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Rational Development of Practical Catalysts for Aromatic Carbon−Nitrogen Bond Formation

21 January 2018

1 reference

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Approaches to catalyst discovery. New carbon–heteroatom and carbon–carbon bond formation

21 January 2018

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Carbon−Heteroatom Bond-Forming Reductive Eliminations of Amines, Ethers, and Sulfides

21 January 2018

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Synthesis and structure-activity study of fungicidal anilinopyrimidines leading to mepanipyrim (KIF-3535) as an anti-Botrytis agent

21 January 2018

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Mepanipyrim, a novel inhibitor of pharmacologically induced Golgi dispersion

21 January 2018

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Regio- and chemoselective magnesiation of protected uracils and thiouracils using TMPMgCl x LiCl and TMP(2)Mg x 2 LiCl

21 January 2018

1 reference

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A Highly Active Catalyst for the Room-Temperature Amination and Suzuki Coupling of Aryl Chlorides

21 January 2018

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Practical Palladium Catalysts for C-N and C-O Bond Formation

21 January 2018

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Development of the Copper-Catalyzed Olefin Aziridination Reaction

21 January 2018

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The oxidation of organocuprates--an offbeat strategy for synthesis

21 January 2018

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A convenient synthesis of acetylenes: catalytic substitutions of acetylenic hydrogen with bromoalkenes, iodoarenes and bromopyridines

21 January 2018

1 reference

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High temperature zincation of functionalized aromatics and heteroaromatics using TMPZnCl.LiCl and microwave irradiation.

21 January 2018

1 reference

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Efficient mono- and bis-functionalization of 3,6-dichloropyridazine using (tmp)2Zn.2MgCl2.2LiCl

21 January 2018

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Imaging in the era of molecular oncology

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The crystal structure of the photoprotein aequorin at 2.3 A resolution

21 January 2018

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Conjugated nitroalkenes: versatile intermediates in organic synthesis

21 January 2018

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Preparation of 5-brominated and 5,5'-dibrominated 2,2'-bipyridines and 2,2'-bipyrimidines

21 January 2018

1 reference

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Direct zincation of functionalized aromatics and heterocycles by using a magnesium base in the presence of ZnCl2.

21 January 2018

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Improved regioselectivity in pyrazole formation through the use of fluorinated alcohols as solvents: synthesis and biological activity of fluorinated tebufenpyrad analogs.

21 January 2018

1 reference

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Synthesis of new fluorinated Tebufenpyrad analogs with acaricidal activity through regioselective pyrazole formation.

21 January 2018

1 reference

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Atom-efficient metal-catalyzed cross-coupling reaction of indium organometallics with organic electrophiles

21 January 2018

1 reference

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Frustrated Lewis Pairs: Metal-free Hydrogen Activation and More

21 January 2018

1 reference

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A study of BF3-promoted ortho lithiation of anilines and DFT calculations on the role of fluorine-lithium interactions

21 January 2018

1 reference

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Palladium-catalyzed Suzuki-Miyaura cross-coupling reactions of potassium aryl- and heteroaryltrifluoroborates

21 January 2018

1 reference

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A general and efficient method for the Suzuki-Miyaura coupling of 2-pyridyl nucleophiles

21 January 2018

1 reference

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Organotrifluoroborates and monocoordinated palladium complexes as catalysts--a perfect combination for Suzuki-Miyaura coupling

21 January 2018

1 reference

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Direct C−H Arylation of Electron-Deficient Heterocycles with Arylboronic Acids

21 January 2018

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Synthesis of dibenzothiophenes and related classes of heterocycles by using functionalized dithiocarbamates

21 January 2018

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Directed manganation of functionalized arenes and heterocycles using tmp2Mn x 2 MgCl2 x 4 LiCl.

21 January 2018

1 reference

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Unmasking Representative Structures of TMP-Active Hauser and Turbo-Hauser Bases

21 January 2018

1 reference

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Modern Ate Chemistry: Applications of Synergic Mixed Alkali-Metal−Magnesium or −Zinc Reagents in Synthesis and Structure Building

21 January 2018

1 reference

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Post-Metalation Structural Insights into the Use of Alkali-Metal-Mediated Zincation for Directedortho-Metalation of a Tertiary Aromatic Amide

21 January 2018

1 reference

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Contacted Ion-Pair Lithium Alkylamidoaluminates: Intramolecular Alumination (Al−H Exchange) Traps for TMEDA and PMDETA

21 January 2018

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Alkali-Metal-Mediated Manganation: A Method for Directly Attaching Manganese(II) Centers to Aromatic Frameworks

21 January 2018

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Sodium-Mediated Manganation: Direct Mono- and Dimanganation of Benzene and Synthesis of a Transition-Metal Inverse-Crown Complex

21 January 2018

1 reference

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Alkali-Metal-Mediated Zincation of Ferrocene: Synthesis, Structure, and Reactivity of a Lithium Tmp/Zincate Reagent

21 January 2018

1 reference

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New reactivity and structural insights of alkali-metal-mediated alumination in directed ortho-alumination of a tertiary aromatic amide

21 January 2018

1 reference

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Lewis base stabilized lithium TMP-aluminates: an unexpected fragmentation and capture reaction involving cyclic ether 1,4-dioxane

21 January 2018

1 reference

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Synergic Monodeprotonation of Bis(benzene)chromium by Using Mixed Alkali Metal-Magnesium Amide Bases and Structural Characterization of the Heterotrimetallic Products

21 January 2018

1 reference

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Synergic Para-Directed Monometalation of Bis(toluene)chromium by Alkali-Metal-Mediated Magnesiation

21 January 2018

1 reference

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Alkali-Metal-Mediated Zincation of Polycyclic Aromatic Hydrocarbons: Synthesis and Structures of Mono- and Dizincated Naphthalenes

21 January 2018

1 reference

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Alkali-Metal-Mediated Zincation of Anisole: Synthesis and Structures of Three Instructive Ortho-Zincated Complexes

21 January 2018

1 reference

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Structurally Defined Reactions of Sodium TMP–Zincate with Nitrile Compounds: Synthesis of a Salt-Like Sodium Sodiumdizincate and Other Unexpected Ion-Pair Products

21 January 2018

1 reference

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Fluorine-Flanked Congested Sites: Minimal, Though Perceptible Buttressing Effects on the Proton Mobility of Arenes

21 January 2018

1 reference

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21 January 2018

Identifiers

DOI

10.1002/ANIE.201101960

1 reference

25 August 2017

1 reference